Modernized Liquid Helium-Free Closed-Cycle Cryostat for Mössbauer Research

S. S. Starchikov; Старчиков С. С.; K. O. Funtov; Фунтов К. О.; V. A. Zayakhanov; Заяханов В. А.; K. V. Frolov; Фролов К. В.; M. G. Klenov; Клёнов М. Г.; I. Yu. Bondarenko; Бондаренко И. Ю.; I. S. Lyubutin; Любутин И. С.

doi:10.31857/S003281622302026X

Modernized Liquid Helium-Free Closed-Cycle Cryostat for Mössbauer Research

Authors: Starchikov S.S.¹, Funtov K.O.¹, Zayakhanov V.A.¹, Frolov K.V.¹, Klenov M.G.², Bondarenko I.Y.², Lyubutin I.S.¹
Affiliations:
1. Shubnikov Institute of Crystallography of Federal Scientific Research Centre “Crystallography and Photonics”, Russian Academy of Sciences
2. ООО CryoPribor
Issue: No 3 (2023)
Pages: 130-141
Section: ЛАБОРАТОРНАЯ ТЕХНИКА
URL: https://rjraap.com/0032-8162/article/view/670530
DOI: https://doi.org/10.31857/S003281622302026X
EDN: https://elibrary.ru/GTURMM
ID: 670530

Cite item

Full Text

Open Access
Restricted Access

Access granted
Restricted Access

Subscription Access

Abstract
About the authors
References
Supplementary files
Statistics

Abstract

One of the problems in the use of closed-cycle cryostats for applied and basic scientific research is the transmission of mechanical vibrations to the sample. This is particularly relevant for Mössbauer spectroscopy and optical research methods since vibrations lead to broadening of spectral lines. This paper presents various engineering approaches to reducing mechanical vibrations on a sample in closed-cycle cryostats, in particular for Mössbauer spectroscopy. The broadening of the spectral lines of the reference absorber, α-Fe foil, was analyzed and a comparison of the spectra of a FeBO3 single crystal of high structural quality before and after updating the cryostat was made. The obtained results can be used to develop new cryostats or improve existing ones.

References

Li X., Zhu K., Pang J., Tian M., Liu J., Rykov A.I., Zheng M., Wang X., Zhu X., Huang Y., Liu B., Wang J., Yang W., Zhang T. // Appl. Catal. B Environ. 2018. V. 224. P. 518. https://doi.org/10.1016/j.apcatb.2017.11.004
Tombácz E., Turcu R., Socoliuc V., Vékás L. // Biochem. Biophys. Res. Commun. 2015. V. 468. № 3. P. 442. https://doi.org/10.1016/j.bbrc.2015.08.030
Oshtrakh M.I. // Cell Biochem. Biophys. 2019. V. 77. № 1. P. 15. https://doi.org/10.1007/s12013-018-0843-8
Chuev M.A., Cherepanov V.M., Deyev S.M., Mischenko I.N., Nikitin M.P., Polikarpov M.A., Panchenko V.Y. // AIP Conference Proceedings. 2010. V. 1311. P. 322. https://doi.org/10.1063/1.3530033
Rusakov V.S., Pokatilov V.S., Sigov A.S., Matsnev M.E., Gubaidulina T.V. // JETP Lett. 2014. V. 100. № 7. P. 463. https://doi.org/10.1134/S0021364014190102
Kuzmann E., Homonnay Z., Klencsár Z. Szalay R. // Molecules. 2021. V. 26. № 4. P. 1062. https://doi.org/10.3390/molecules26041062
Maksimova A.A., Klencsár Z., Oshtrakh M.I., Petrova E.V., Grokhovsky V.I., Kuzmann E., Homonnay Z., Semion-kin V.A. // Hyperfine Interact. 2016. V. 237. № 1. P. 33. https://doi.org/10.1007/s10751-016-1218-4
Sumanov V.D., Aksyonov D.A., Drozhzhin O.A., Presniakov I., Sobolev A.V., Glazkova I., Tsirlin A.A., Rupasov D., Senyshyn A., Kolesnik I.V., Stevenson K.J., Antipov E., Abakumov A.M. // Chem. Mater. 2019. V. 31. № 14. P. 5035. https://doi.org/10.1021/acs.chemmater.9b00627
Shen G., Mao H.K. // Reports Prog. Phys. 2017. V. 80. № 1. P. 016101. https://doi.org/10.1088/1361-6633/80/1/016101
Williams J.M. // Cryogenics (Guildf). 1975. V. 15. № 6. P. 307. https://doi.org/10.1016/0011-2275(75)90077-6
Micke P., Stark J., King S.A., Leopold T., Pfeifer T., Schmöger L., Schwarz M., Spieß L.J., Schmidt P.O., Crespo López-Urrutia J.R. // Rev. Sci. Instrum. 2019. V. 90. № 6. P. 065104. https://doi.org/10.1063/1.5088593
Ekin J. Experimental techniques for low-temperature measurements: cryostat design, material properties and superconductor critical-current testing. NY.: Oxford U. Press, 2006. ISBN 978-0-19-857054-7. https://doi.org/10.1063/1.2743130
Gifford W.E. Advances in Cryogenic Engineering. Boston, MA: Springer US, 1966. P. 152–159.
D’Addabbo A., Bucci C., Canonica L., Di Domizio S., Gorla P., Marini L., Nucciotti A., Nutini I., Rusconi C., Welliver B. // Cryogenics (Guildf). 2018. V. 93. P. 56. https://doi.org/10.1016/j.cryogenics.2018.05.001
Ikushima Y., Li R., Tomaru T., Sato N., Suzuki T., Haruyama T., Shintomi T., Yamamoto A. // Cryogenics (Guildf). 2008. V. 48. № 9–10. P. 406. https://doi.org/10.1016/j.cryogenics.2008.04.001
Boolchand P., Lemon G.H., Bresser W.J., Enzweiler R.N., Harris R. // Rev. Sci. Instrum. 1995. V. 66. № 4. P. 3051. https://doi.org/10.1063/1.1145528
Olivieri E., Billard J., De Jesus M., Juillard A. Leder A. // Nucl. Instrum. and Methods Phys. Res. Sect. A Accel. Spectrometers, Detect. Assoc. Equip. 2017. V. 858. P. 73. https://doi.org/10.1016/j.nima.2017.03.045
Наумов П.Г., Любутин И.С., Фролов К.В., Деми-хов Е.И. // ПТЭ. 2010. № 5. С. 158.
Криомагнитные системы tSTAT310x. URL: http://cryo.ru/index.php?option=com_content&task= view&id=72&lang=ru.
Courts S.S. // IOP Conf. Ser. Mater. Sci. Eng. 2017. V. 278. № 1. P. 012076. https://doi.org/10.1088/1757-899X/278/1/012076
Matsnev M.E., Rusakov V.S. // AIP Conference Proceedings. 2012. V. 1489. P. 178. https://doi.org/10.1063/1.4759488
Yagupov S., Strugatsky M., Seleznyova K., Mogilenec Y., Snegirev N., Marchenkov N V., Kulikov A.G., Eliovich Y.A., Frolov K.V., Ogarkova Y.L., Lyubutin I.S. // Cryst. Growth Des. 2018. V. 18. № 12. P. 7435. https://doi.org/10.1021/acs.cgd.8b01128
Lyubutin I.S., Snegirev N.I., Chuev M.A., Starchikov S.S., Smirnova E.S., Lyubutina M.V., Yagupov S.V., Strugatsky M.B., Alekseeva O.A. // J. Alloys Compd. 2022. V. 906. P. 164348. https://doi.org/10.1016/j.jallcom.2022.164348